DEPARTMENT OF CHEMISTRY

Dr. Rafik Rajjak Shaikh

Designation:Assistant Professor
Nature of Employment:Regular
Qualification:Ph.D
Phone:+91 44 2275 1347 ext. 402(Office)
Email ID:rafik.shaikh@crescent.education

Teaching

Educational Background

DegreeDisciplineYear of PassingUniversity
Ph.D.Chemical Sciences2010University of Camerino, Italy
M.Sc.Chemical Sciences2006SRTM University, Maharashtra
B.Sc.Chemistry, Physics, Comp. Sci.2004SRTM University, Maharashtra

Work Experience

DesignationInstitutionDurationNo. of Years
Assistant ProfessorB.S.Abdur Rahman Crescent Institute of Science and Technology, IndiaSep. 2018 to till dateTill date
NRCT Foreign ResearcherVidyasirimedhi Institute of Science and Technology, ThailandJuly 2016 to July 20182 years
Research AssociateJilin University, ChinaJune 2015 to May 20161 year
Inspire FacultyCentral University of Rajasthan, IndiaJune 2013 to September 20141 year 3 months
KCC PostDoc FellowKing Abdulllah University of Science and Technology, Saudi ArabiaJune 2012 to May 20131 year
Alexander von Humboldt FellowTechnical University of Dresden, GermanyFebruary 2011 to May 20121 year 4 months

Collaborative / Adjunct Teaching

DesignationInstitutionYearDuration
KVYTA Tutor  KAUST Virtual Young Talent Academy, King Abdullah University of Science and Technology, Saudi Arabia.2021July-August 2021
2020June-July 2020
SRSI TutorSaudi Research Science Institute, King Abdullah University of Science and Technology, Saudi Arabia.2019June-August 2019
2018July-August 2018
2017July-August 2017

Lecture Courses

  • Green Chemistry
  • Synthetic Organic Chemistry
  • General Chemistry
  • Environmental Studies

Research

Area of Research Interest

  • Synthetic Organic Chemistry
  • Catalysis
  • Green Chemistry and Sustainability
  • Renewable Resources to Value-Added Products
  • Waste-to-Energy

Research Supervision

CoursePh.D.M.Sc. Chemistry
Completed03
Ongoing15
Publications
Publication DetailsJournal Impact Factor
R. R. Shaikh,* S. Thenmozhi: Organocatalytic Upgrading of Biomass-derived Furaldehydes: An Emerging Chemical Technology for Biorefineries. Synthetic Communications (2023), accepted and in press. 
R. Jan, C. A. Biji, K. Shakeela, R. R. Shaikh and G. R. Rao: Green Synthesis of Cyclic Carbonates from Epoxides and CO2 Using Transition Metal Substituted Polyoxometalate-PDDA Hybrid Catalysts. Catalysis Letters (2023). https://doi.org/10.1007/s10562-023-04392-1 
Serajul Haque, M. Abdur Rahman, Rafik Rajjak Shaikh, N. Sirajudeen, Mohamed Bak Kamaludeen, Omprakash Sahu, Effect of powder metallurgy process parameters on tribology and micro hardness of Al6063-nano Al2O3 MMCs, Materials Today: Proceedings, 2022, ISSN 2214-7853, DOI:10.1016/j.matpr.2022.08.255 
Sivasubramanian Pandiarajan, Nallamohamed Hajarabeevi, Rafik Rajjak Shaikh, Sathya Raghunathan, Davoodbasha MubarakAli, Synthesis and Characterization of Novel Schiff Bases Derived from 2-Butyl-4-chloro Imidazole for the Enhanced Antimicrobial Property, Applied Biochemistry and Biotechnology, 2022, DOI: 10.1007/s12010-022-04112-2 
Shaikh, R. R.,* Khan, R. A., Alsalme, A.Highly Product-selective and Scalable Rare-Earth Metal-Catalyzed Meinwald Rearrangement of Epoxy Oleochemicals Under Solvent-free Conditions. Journal of Industrial and Engineering Chemistry, 2018, 64, 446-452.4.841
Shaikh, R. R., Pornpraprom, S. and D’Elia, V.Catalytic strategies for the cycloaddition of pure, diluted and waste CO2 to epoxides under ambient conditions. ACS Catalysis, 20188, 419-450.11.384
Natongchai, W.,Khan, R. A., Alsalme, A., Shaikh, R. R.*YCl3-Catalyzed Highly Selective Ring Opening of Epoxides by Amines at Room Temperature and Under Solvent-Free Conditions. Catalysts, 2017, 7, 340.3.465
Shaikh, R. R.*: Achieving elusive transformations with organocatalysis: direct β-carbon activation of saturated carbonyl compounds, Turkish Journal of Chemistry, 2017, 41, 601-618.1.377
Shaikh, R. R. †, Cuhawijay, S. †, Qian,H., Zhang, Y., Meguellati, K. , Yang, Y.-W.:Biological and related applications of pillar[n]arenes. Chem. Commun. 2017,53, 677-696(†=co-first author)6.29
Xi, L., Shaikh, R. R.*, Du, X.-S., Novack, D., Meguellati, K.*: First Description of a Guanidine-embedded Pillar[5]arene: Opening New Avenues for Biological Applications.Mediterranean Journal of Chemistry 2017, 6, 49-52.NA
Shaikh, I. R., Shaikh, R. A., Shaikh, A. A., WarJ. A., Hangirgekar, S. P., Shaikh, A. L., Shaikh, P. R., Shaikh, R. R.: H-ZSM-5 Zeolite Synthesis by Sourcing Silica from the Wheat Husk Ash:  Characterization and Application as A Versatile Heterogeneous Catalyst in Organic Transformations including Some Multi-Component Reactions. Journal of Catalysts. 2015, 14 pages (2015).NA
Bouhrara, M., Ranga, C., Fihri, A., Shaikh, R. R., Sarawade, P., Emwas, A.-H., Hedhilia, M. N. and Polshettiwar, V.: Nitridated Fibrous Silica (KCC-1) as a Sustainable Solid Base Nanocatalyst. ACS Sustainable Chem. & Eng. 2013, 1, 1192-1199 (Front Cover).6.140
Palmieri, A., Petrini, M., and Shaikh, R. R.: Synthesis of 3-Substituted Indoles via Reactive Alkylideneindolenine Intermediates. Org. Biomol. Chem.2010, 8, 1259–1270.3.423
Petrini, M., and Shaikh, R. R.: A “Click” Approach to the Synthesis of 3-[2-(1-Alkyltriazol-4-yl) ethyl]indoles. Synthesis2009, 18, 3143-3149.2.722
Shaikh, R. R., Mazzanti, A., Petrini, M., Bartoli, G., and Melchiorre, P.: Proline Catalyzed Asymmetric Formal α-Alkylation of Aldehydes via vinylogous Iminium Ion Intermediate Generated from ArylsulfonylIndoles. Angew. Chem. Int. Ed. 2008, 47, 8707–8710. (Highlighted in:Angew. Chem. Int. Ed. 2011, 50, 12146-12147).12.102
Palmieri, A., Petrini, M., and Shaikh, R. R.: Double Functionalization of N-Boc-3-(Tosylmethyl)indole Exploiting the Activating Properties of the Tosyl Group.Synlett2008, 12, 1845-1851.2.369
Petrini, M., and Shaikh, R. R.: Synthesis of Indolylalkylphosphonates and 3-(1-Diphenylphosphinoalkyl) Indoles by Reaction of 3-(1-Arylsulfonylalkyl) Indoles with Phosphorus Derivatives. Tetrahedron Letters, 2008, 49, 5645–5648.2.125
Ballini, R., Palmieri, A., Petrini, M., and Shaikh, R. R.: Reaction of 3-(1-Arylsulfonylalkyl) Indoles with Easily Enolisable Derivatives Promoted by Potassium Fluoride on Basic Alumina. Adv. Synth. Catal.2008, 350, 129 – 134.5.123
Shaikh, I., Shaikh, P., Shaikh, R. R.: Synthesis and Biological Activity of Some Thiazine Substituted Benzoxazoles.Int. J. Chem. Sci., 2005, 3, 403-406.NA

Conference Abstracts / Papers / Theses

  • SMART-2020: Smart Materials and their Applications in Recent Technologies (2020): “Keggin-Structured Heteropolyacids-Catalyzed Highly Efficient Synthesis of Oxime at Mild Condition”, 4-5 March, 2020, Periyar University, Tamil Nadu, India.
  • SMART-2020: Smart Materials and their Applications in Recent Technologies (2020): “Highly Regioselective Ring Opening of Epoxides by Amines at Room Temperature Using AKeggin-Structured Heteropolyacids-based Catalyst”, 4-5 March, 2020, Periyar University, Tamil Nadu, India.
  • PPC and PETROMAT Symposium (2017): “Novel Cyclic Carbonate-based Organic Molecules via carbon dioxide Fixation”, 23 May, 2017, Bangkok, Thailand
  • Humboldt KollegLavasa-Surface Science and Engineered Surfaces (2014) “Engineering nanoparticle based heterogeneous catalysts- a sustainable approach to develop industrially useful chemical processes“, 14-16 February, 2014, Lavasa, Maharashtra, India.
  • 101st Indian Science Congress-2014 Jammu (2014) “Nitridated Fibrous Nano-Silicaas a Sustainable Solid Base Catalyst”, University of Jammu, Jammu, India.
  • University of Camerino, Italy (2010) Synthesis of 3-Substituted Indoles via Alkylideneindolenine Intermediates Generated from Arylsulfonylalkyl Indoles. (PhD Thesis).
  • 23rd European Colloquium on Heterocyclic Chemistry (2008) “A New Approach to the Synthesis of 3-Substituted Indoles”;September 9-13, 2008, Antwerp, Belgium.
  • National Chemical Laboratory, (2006): Diastereoselective Synthesis of β-Lactam Using D-glucose Derived Chiral Imine. (MSc thesis submitted to SRTM University, India).

Sponsored Projects

GRANTSponsoring Body/OrganizationSanctioned Amount (in lakhs)Project Duration
CRESCENT SEED GrantB.S.Abdur Rahman Crescent Institute of Science and Technology, India0.25January 2020-December 2021
CPSF GrantChina Postdoctoral Science Foundation, China5July 2015-June 2016
INSPIRE GrantDepartment of Science and Technology (DST), India7June 2013-September 2014

Membership / Affiliations

  • Member, National Graphene Association, USA.
  • Life Member, Indian Science Congress Association (ISCA), INDIA.
  • Life Member, Chemical Research Society of India (CRSI), INDIA.
  • Alumni, Alexander von Humboldt Foundation, Germany.
  • Review Editor, Frontiers in Energy Research
  • Review Editor, Frontiers in Bioengineering and Biotechnology